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    Author(s): S. Nami Kartal; Frederick Green
    Date: 2002
    Source: Forest products journal. Vol. 52, no. 6 (June 2002): Pages 75-79
    Publication Series: Miscellaneous Publication
    PDF: View PDF  (198 KB)

    Description

    This paper describes the development of a microsssay for boron and the application of this microassay for evaluating leachability of boron by post-treatment of southern pine with the calcium precipitating agent NHA (N'N-napthaloylhydroxylamine). The microsssay method for quantitative estimation of boron content in treated wood and leachates is a microadaptation of the colorimetric azomethine-H method. The primary advantages of this microassay method are that it uses fewer reagents, uses smaller sample volumes, and conserves time for analysis when a large number of tests are required. Wood blocks were treated with boric acid, disodium octaborate tetrahydrate (DOT), and NHA solutions at several concentrations. Boron leaching performance was evaluated on the blocks using AWPA E11-97 standard method. Blocks treated sequentially with DOT and then with 0.5 or 1.0 percent NHA solutions showed -30% less boron leaching, whereas similar treatment with boric acid and 0.1% NHA solutions did not enhance boron retention compared with the blocks treated with only boric acid. We conclude that precipitation of NHA at higher concentrations decreases or limits boron leaching.

    Publication Notes

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    • This article was written and prepared by U.S. Government employees on official time, and is therefore in the public domain.

    Citation

    Kartal, S. Nami; Green, Frederick 2002. Development and application of colorimetric microassay for determining boron-containing compounds. Forest products journal. Vol. 52, no. 6 (June 2002): Pages 75-79

    Keywords

    Calorimetric microassays, boron compounds, microassays

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